Crystal and Molecular Structure of 3-Hydrazino-1- Hydrazinothio- Carbonyl Pyrazoline (TNT3)
(2000). Crystal and Molecular Structure of 3-Hydrazino-1- Hydrazinothio- Carbonyl Pyrazoline (TNT3). EKB Journal Management System, 23(2), 251-258. doi: 10.21608/ejs.2000.151733
. "Crystal and Molecular Structure of 3-Hydrazino-1- Hydrazinothio- Carbonyl Pyrazoline (TNT3)". EKB Journal Management System, 23, 2, 2000, 251-258. doi: 10.21608/ejs.2000.151733
(2000). 'Crystal and Molecular Structure of 3-Hydrazino-1- Hydrazinothio- Carbonyl Pyrazoline (TNT3)', EKB Journal Management System, 23(2), pp. 251-258. doi: 10.21608/ejs.2000.151733
Crystal and Molecular Structure of 3-Hydrazino-1- Hydrazinothio- Carbonyl Pyrazoline (TNT3). EKB Journal Management System, 2000; 23(2): 251-258. doi: 10.21608/ejs.2000.151733

Crystal and Molecular Structure of 3-Hydrazino-1- Hydrazinothio- Carbonyl Pyrazoline (TNT3)

Egyptian Journal of Solids
Article 6, Volume 23, Issue 2, 2000, Pages 251-258    PDF (135.49 K)
DOI: 10.21608/ejs.2000.151733
Abstract
The crystal and molecular structure of 3-Hydrazino-1-Hydrazinothiocarbonyl
pyrazoline (TNT3), C4H10N6S has been determined with MoKαα
diffractometer data by direct methods. The compound crystallized in the
monoclinic space group P21/c, with a = 6.925(1), b=13.675(3), c=8.190(2)Ǻ
and β=108.14(3)º. The structure was refined by full matrix least squares
methods to R=0.047 using 917 reflections. The pyrazoline ring was found to be
planner and delocalized. The amino groups connected to N7 and to N9 is
extended and trans.
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