PREPARATION AND REACTIVITY OF SOME NEW DIAZAPHOSPHOLINE COMPOUNDS | ||||
Al-Azhar Bulletin of Science | ||||
Article 5, Volume 17, Issue 2-A, December 2006, Page 73-78 PDF (319.37 K) | ||||
Document Type: Original Article | ||||
DOI: 10.21608/absb.2006.11654 | ||||
View on SCiNiTO | ||||
Authors | ||||
A. M. ALAGHAZ* ; H. A. GUMAA | ||||
Chemistry Department, Faculty of Science (Boys), Al-Azhar University, Nasr-City, Cairo, Egypt | ||||
Abstract | ||||
A reaction of cyclohexanone phenylhydrazone with (het)aryldihalogenophosphines has been studied. Cyclohexanone phenylhydrazone reacts with phenyldichlorophosphine and 5- methyl-2-furyldichlorophosphine to provide the corresponding 1,2,3 diazaphospholines derivatives in high yields. These compounds (3-7) have been characterized by microanalytical, FT-IR, MS, 1H, and 31P-NMR, and UV spectra. | ||||
Keywords | ||||
cyclohexanone; phenylhydrazone; phenyldichlorophosphine; diazaphospholines | ||||
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