Synthesis and Photooxygenation of Angular Furoquinolinone. | ||||
MEJ- Mansoura Engineering Journal | ||||
Article 9, Volume 37, Issue 1, March 2012, Page 1-11 PDF (284.66 K) | ||||
Document Type: Research Studies | ||||
DOI: 10.21608/bfemu.2020.119918 | ||||
View on SCiNiTO | ||||
Authors | ||||
Sameh El_Gogary 1; Hoda Hassan2; Mohammad Mohammad Mashaly2 | ||||
1Department of Chemistry, Faculty of Science at (New) Damietta., Mansoura University., Egypt. | ||||
2Department of Chemistry, Faculty of Science at (New) Damietta, Mansoura University, Egypt | ||||
Abstract | ||||
Synthesis of 4,8,9-trimethylfuro[2,3-h]quinolin-2(1H)-one as angular furoquinolinone (psoralen analog) was carried out through Williamson reaction of 7-hydroxy-4-methyl-2H-quinolin-2-one with 3 chloro-2-butanone followed by cyclization with polyphosphoric acid (PPA).o- Benzoylhydroxy derivative of quinolinone was prepared through the photooxygenation and Fries rearrangement. | ||||
Keywords | ||||
Furocoumarin; Psoralen; Photooxygenation and Fries REARRANGEMENT | ||||
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