Crystal and Molecular Structure of 3-Hydrazino-1- Hydrazinothio- Carbonyl Pyrazoline (TNT3) | ||||
Egyptian Journal of Solids | ||||
Article 6, Volume 23, Issue 2, 2000, Page 251-258 PDF (135.49 K) | ||||
DOI: 10.21608/ejs.2000.151733 | ||||
View on SCiNiTO | ||||
Abstract | ||||
The crystal and molecular structure of 3-Hydrazino-1-Hydrazinothiocarbonyl pyrazoline (TNT3), C4H10N6S has been determined with MoKαα diffractometer data by direct methods. The compound crystallized in the monoclinic space group P21/c, with a = 6.925(1), b=13.675(3), c=8.190(2)Ǻ and β=108.14(3)º. The structure was refined by full matrix least squares methods to R=0.047 using 917 reflections. The pyrazoline ring was found to be planner and delocalized. The amino groups connected to N7 and to N9 is extended and trans. | ||||
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