Synthesis and Characterization of Bis-azo 1,2,4,5-Tetrazine Dyestuff | ||||
| Journal of Textiles, Coloration and Polymer Science | ||||
| Article 3, Volume 15, Issue 1, December 2018, Page 33-36 PDF (517.16 K) | ||||
| Document Type: Original Article | ||||
| DOI: 10.21608/jtcps.2018.5033.1003 | ||||
 View on SCiNiTO | ||||
| Authors | ||||
Tawfik A. Khattab   ; Mohamed Rehan
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| National Research Centre | ||||
| Abstract | ||||
| The design, synthesis and characterization of symmetrical 3,6-Bis(2-(4-(dodecyloxy)phenyl)-1-(4-(phenyl)diazene)-1,2,4,5-tetrazine are described. The novel sym-tetrazine was prepared by addition reaction of 4-(2-(4-decyloxyphenyl)diazenyl)benzonitrile with hydrazine monohydrate followed by oxidation reaction to afford the corresponding bis(azo)-1,2,4,5-tetrazine. The chemical structure of the sym-tetrazine compound was confirmed by elemental analysis, fourier-transform infrared spectroscopy (FT-IR), and nuclear magnetic resonance (1H and 13C NMR) spectral measurements. The design, synthesis and characterization of symmetrical 3,6-Bis(2-(4-(dodecyloxy)phenyl)-1-(4-(phenyl)diazene)-1,2,4,5-tetrazine are described. The novel sym-tetrazine was prepared by addition reaction of 4-(2-(4-decyloxyphenyl)diazenyl)benzonitrile with hydrazine monohydrate followed by oxidation reaction to afford the corresponding bis(azo)-1,2,4,5-tetrazine. The chemical structure of the sym-tetrazine compound was confirmed by elemental analysis, fourier-transform infrared spectroscopy (FT-IR), and nuclear magnetic resonance (1H and 13C NMR) spectral measurements. | ||||
| Keywords | ||||
| sym-Tetrazine; Bis-azo; Disperse dye | ||||
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