Preparation and Characterization of some Polyalkylarylamines.
Shaaban, A., El-Komy, M., Al-Sarwy, A., Rashed, I. (2021). Preparation and Characterization of some Polyalkylarylamines.. EKB Journal Management System, 13(2), 27-37. doi: 10.21608/bfemu.2021.173266
A. Shaaban; M. A. El-Komy; A. A. Al-Sarwy; I. Gar Al-Alam Rashed. "Preparation and Characterization of some Polyalkylarylamines.". EKB Journal Management System, 13, 2, 2021, 27-37. doi: 10.21608/bfemu.2021.173266
Shaaban, A., El-Komy, M., Al-Sarwy, A., Rashed, I. (2021). 'Preparation and Characterization of some Polyalkylarylamines.', EKB Journal Management System, 13(2), pp. 27-37. doi: 10.21608/bfemu.2021.173266
Shaaban, A., El-Komy, M., Al-Sarwy, A., Rashed, I. Preparation and Characterization of some Polyalkylarylamines.. EKB Journal Management System, 2021; 13(2): 27-37. doi: 10.21608/bfemu.2021.173266

Preparation and Characterization of some Polyalkylarylamines.

MEJ- Mansoura Engineering Journal
Article 18, Volume 13, Issue 2, December 1988, Page 27-37  XML PDF (569.87 K)
Document Type: Research Studies
DOI: 10.21608/bfemu.2021.173266
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Authors
A. Shaaban1; M. A. El-Komy2; A. A. Al-Sarwy2; I. Gar Al-Alam Rashed* 3
1Department of Chemistry., Faculty of Science., Zagazig University (Benha Branch)., Benha., Egypt.
2Department of Physical and Mathematical Science., Faculty of Engineering (Shoubra)., Zagazig University., (Benno Branch., Cairo., Egypt.
3Associate Professor., Department of Physical Science., Faculty of Engineering., Mansoura University., El-Mansoura., Egypt.
Abstract
Adducts of polyalkylarylamines will stoichiometric amounts of stannous chloride were obtained by the reaction of 1,2-dichloroethane with m-phenylenediamine, p-phenylenediamine and 4,4 diaminodiphenyl in the presence of hydrochloric acid and stoichiometric amounts of stannous chloride in methanol as a solvent. Also, adduct of poly (chloromethyne-co- 4,4-dianiinodiphenyl) was obtained from the reaction of chloroform and benzidine by similar method. The structure of these adducts was confirmed by JR spectroscopy, as well 0.X-ray diffractometery, These adducts when reacted with aqueous solution of ammonium carbonate gave the corresponding polyalkylaryl-amine hydrochlorides. Also thermal analysis of these adducts were carried out . 
 
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