Synthesis and Characterization of Some Transition Metal Complexes with Bis(o-aminophenyl)Disulfide Alkane Ligands | ||||
| Egyptian Journal of Chemistry | ||||
| Article 65, Volume 64, Issue 11, November 2021, Page 6821-6826 PDF (676.53 K) | ||||
| Document Type: Original Article | ||||
| DOI: 10.21608/ejchem.2021.78022.3815 | ||||
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| Authors | ||||
| E.M. Salih1; F.T. Saeed2 | ||||
| 1Senior Laboratory assistant in AL-Mutamyzeen Secondary School Mosul-Iraq | ||||
| 2Department of chemistry Colloge of science Mosul University | ||||
| Abstract | ||||
| A series of new complexes of the type [M(L)Cl2] and [M(L)]Cl2 where M= Co(II),Ni(II) and Cu(II), L=L1 or L2 {L1= 1,2-Bis(o-aminophenyl)disulfide propane, L2=1,2-Bis(o- aminophenyl)disulfide butane, have been prepared in 1:1 (L:M) and characterized by molar conductance , magnetic moment,FT-IR,1H-NMR , Uv-visible spectra studies and metal content analysis. Conductivity data in DMF and DMSO solution showed that some complexes are non-electrolyte and others are electrolyte . Magnetic moment and electronic spectra indicate that some of the complexes have a tetrahedral and the others have an square planar environment. | ||||
| Keywords | ||||
| 1; 2-Bis(o-aminophenyl)disulfide derivatives; metal complexes; spectral study | ||||
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