Synthesis, structural characterization, and antibacterial studies of new borate 13-93B3 bioglasses with low copper dopant
Elmowafy, B., Abdelghany, A., Ramadan, R., Ghazy, R., Meaz, T. (2022). Synthesis, structural characterization, and antibacterial studies of new borate 13-93B3 bioglasses with low copper dopant. EKB Journal Management System, 65(9), 1-10. doi: 10.21608/ejchem.2022.84829.4137
Bothina Mohammed Elmowafy; Amr Abdelghany; Rawya Mohammed Ramadan; R Ghazy; T. Meaz. "Synthesis, structural characterization, and antibacterial studies of new borate 13-93B3 bioglasses with low copper dopant". EKB Journal Management System, 65, 9, 2022, 1-10. doi: 10.21608/ejchem.2022.84829.4137
Elmowafy, B., Abdelghany, A., Ramadan, R., Ghazy, R., Meaz, T. (2022). 'Synthesis, structural characterization, and antibacterial studies of new borate 13-93B3 bioglasses with low copper dopant', EKB Journal Management System, 65(9), pp. 1-10. doi: 10.21608/ejchem.2022.84829.4137
Elmowafy, B., Abdelghany, A., Ramadan, R., Ghazy, R., Meaz, T. Synthesis, structural characterization, and antibacterial studies of new borate 13-93B3 bioglasses with low copper dopant. EKB Journal Management System, 2022; 65(9): 1-10. doi: 10.21608/ejchem.2022.84829.4137

Synthesis, structural characterization, and antibacterial studies of new borate 13-93B3 bioglasses with low copper dopant

Egyptian Journal of Chemistry
Article 1, Volume 65, Issue 9, September 2022, Page 1-10  XML PDF (574.18 K)
Document Type: Original Article
DOI: 10.21608/ejchem.2022.84829.4137
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Authors
Bothina Mohammed Elmowafy email orcid 1; Amr Abdelghanyorcid 2; Rawya Mohammed Ramadanorcid 3; R Ghazy4; T. Meaz4
1Biophysics, Faculty of science, Mansoura University, Alexandria, Egypt
2Spectroscopy Department, National Research Centre, Dokki, Cairo, Egypt
3National Research Centre (NRC)
4Physics Department, Faculty of Science, Tanta University, Tanta, Egypt
Abstract
Glasses of nominal composition (6Na2O.12K2O.5MgO.20CaO.4P2O5.(53-x) B2O3. xCuO Wt%) (0 ≤ x ≤ 0.6 wt%) were successfully synthesized via the traditional melt quenching route. The synthesized samples proved to be amorphous without any tendency for crystallization through X-ray diffraction measurements. Structural changes within the glassy matrix and their ability for bone bonding were investigated through employing deconvolution analysis technique (DAT) combined with Fourier transform Infrared (FT-IR) spectral measurement to calculate the percent of tetrahedral boron change versus doping copper ion concentration. It was found that copper additions control the transformation of triangular and tetrahedral coordinated boron that increase with increasing copper content up to 0.4 wt%. UV/Vis. electronic spectral data was used to calculate physical parameters including optical energy gap, refractive index, dielectric permittivity, and other physical parameters. Antimicrobial activity against different pathogenic grams using a cup and disc diffusion method was also correlated to the copper oxide doping level. All previous investigations were used as an optimizing factor for the synthesis of bioactive borate glass suitable for wound healing and wound dressing applications.
Keywords
113-93B3 Bioglass; Antimicrobial studies; copper oxide; melt quenching; structural chracterization
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