Synthesis of new compounds of (5E,5'E)-5,5'-([1,1'-biphenyl]-4,4'-diylbis(azanylylidene))bis (3,3-dimethylcyclohexan-1-one) in new laboratory methods
Farhan, M., Younis, A. (2022). Synthesis of new compounds of (5E,5'E)-5,5'-([1,1'-biphenyl]-4,4'-diylbis(azanylylidene))bis (3,3-dimethylcyclohexan-1-one) in new laboratory methods. EKB Journal Management System, 65(10), 515-522. doi: 10.21608/ejchem.2022.120507.5404
Marwan M. Farhan; Atyaf A Younis. "Synthesis of new compounds of (5E,5'E)-5,5'-([1,1'-biphenyl]-4,4'-diylbis(azanylylidene))bis (3,3-dimethylcyclohexan-1-one) in new laboratory methods". EKB Journal Management System, 65, 10, 2022, 515-522. doi: 10.21608/ejchem.2022.120507.5404
Farhan, M., Younis, A. (2022). 'Synthesis of new compounds of (5E,5'E)-5,5'-([1,1'-biphenyl]-4,4'-diylbis(azanylylidene))bis (3,3-dimethylcyclohexan-1-one) in new laboratory methods', EKB Journal Management System, 65(10), pp. 515-522. doi: 10.21608/ejchem.2022.120507.5404
Farhan, M., Younis, A. Synthesis of new compounds of (5E,5'E)-5,5'-([1,1'-biphenyl]-4,4'-diylbis(azanylylidene))bis (3,3-dimethylcyclohexan-1-one) in new laboratory methods. EKB Journal Management System, 2022; 65(10): 515-522. doi: 10.21608/ejchem.2022.120507.5404

Synthesis of new compounds of (5E,5'E)-5,5'-([1,1'-biphenyl]-4,4'-diylbis(azanylylidene))bis (3,3-dimethylcyclohexan-1-one) in new laboratory methods

Egyptian Journal of Chemistry
Article 48, Volume 65, Issue 10, October 2022, Page 515-522  XML PDF (610.31 K)
Document Type: Original Article
DOI: 10.21608/ejchem.2022.120507.5404
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Authors
Marwan M. Farhan email 1; Atyaf A Younis2
1University of Anbar, College of Applied Science, Hit, Iraq.
2University of Anbar, College of Applied Science, Hit, Iraq
Abstract
Six new Schiff bases were synthesized via reaction of benzidine, [1,1'-biphenyl]-4,4'-diyldimethanamine, 3,3'-dimethyl-[1,1'-biphenyl]-4,4'-diamine, 2,2'-dimethyl-[1,1'-biphenyl]-4,4'-diamine, ethane-1,2-diamine and propane-1,3-diamine with 5,5-dimethylcyclohexane-1,3-dione in acidic medium of acetic acid. The structures of new compounds were elucidated with NMR, FTIR, UV and elemental analysis and antimicrobial activity of them were applied. Three different methods were used Conventional, microwave and grinding methods, and concluded that the grinding and clicking method is the best in terms of the quantity of the product and the time required for the reaction to be very fast, As well as protecting the health of workers and the environment.
Keywords
Bis-Schiff bases; Ecofriendly method; antimicrobial activity
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