Synthesis and characterization of barium hexaferrite (BaFe12O19) nanoparticles from iron ore waste and their possible application in water treatment | ||||
| The International Conference on Chemical and Environmental Engineering | ||||
| Volume 10, Issue 10, July 2020, Page 1-14 PDF (855.15 K) | ||||
| Document Type: Original Article | ||||
| DOI: 10.1088/1757-899X/975/1/012002 | ||||
 View on SCiNiTO | ||||
| Authors | ||||
Nehal A. Erfan  1; Salwa A. M. Abdel-Hameed2; Asma A. Mohammed1
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| 1Chemical engineering department, faculty of engineering, Minia university, Minia, Egypt. | ||||
| 2Glass Research Department, National Research Centre, Dokki, Cairo, Egypt. | ||||
| Abstract | ||||
| In this work hard magnetic glass ceramics has been fabricated using Egyptian Bahariya oasis ore; which contains not less than 51% of its weight as pure iron. High energy planetary ball mill was used to convert the prepared magnetic sample into nanoparticles. Different mechanical milling times were applied to study its effect on the properties of the produced magnetic glass ceramic. Scanning electron microscope (SEM), transmission electron microscope (TEM), X-ray florescence analysis (XRF), differential thermal analysis (DTA), X-ray diffraction analysis (XRD), Raman spectroscopy and Vibrating sample magnetometer (VSM) analysis techniques were performed to characterize the prepared glass ceramic samples before and after exposing to mechanical milling process. XRD revealed crystallization of barium hexaferrite as major phase with average crystallite size ~26 nm. Saturation magnetization Ms depicted 21.2 emu/g after 5 hours milling. The produces nanoparticles after 5 hours milling showed a good performance in removal of pollutants like methylene blue and Congo red from water by adsorption. | ||||
| Keywords | ||||
| Magnetic glass ceramics; Ball milling; Barium hexaferrite; nanoparticles; Iron ore, Waste; Recycling | ||||
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