New Luminol Azo 1-(4 -sulfophenyl)-3-methyl-5- pyrazolone Reagent Preparation, Characterization, Biological Effectiveness and Enhancement Studies
Taha, H., Mohammed, H. (2023). New Luminol Azo 1-(4 -sulfophenyl)-3-methyl-5- pyrazolone Reagent Preparation, Characterization, Biological Effectiveness and Enhancement Studies. EKB Journal Management System, 15(2), 253-266. doi: 10.21608/eajbsc.2023.316153
Hanaa K. A. Taha; Hussain J. Mohammed. "New Luminol Azo 1-(4 -sulfophenyl)-3-methyl-5- pyrazolone Reagent Preparation, Characterization, Biological Effectiveness and Enhancement Studies". EKB Journal Management System, 15, 2, 2023, 253-266. doi: 10.21608/eajbsc.2023.316153
Taha, H., Mohammed, H. (2023). 'New Luminol Azo 1-(4 -sulfophenyl)-3-methyl-5- pyrazolone Reagent Preparation, Characterization, Biological Effectiveness and Enhancement Studies', EKB Journal Management System, 15(2), pp. 253-266. doi: 10.21608/eajbsc.2023.316153
Taha, H., Mohammed, H. New Luminol Azo 1-(4 -sulfophenyl)-3-methyl-5- pyrazolone Reagent Preparation, Characterization, Biological Effectiveness and Enhancement Studies. EKB Journal Management System, 2023; 15(2): 253-266. doi: 10.21608/eajbsc.2023.316153

New Luminol Azo 1-(4 -sulfophenyl)-3-methyl-5- pyrazolone Reagent Preparation, Characterization, Biological Effectiveness and Enhancement Studies

Egyptian Academic Journal of Biological Sciences. C, Physiology and Molecular Biology
Volume 15, Issue 2, December 2023, Page 253-266  XML PDF (1.33 MB)
Document Type: Original Article
DOI: 10.21608/eajbsc.2023.316153
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Authors
Hanaa K. A. Taha; Hussain J. Mohammed
Chemistry Department / Faculty of Science / Kufa University
Abstract
A new azo dye was produced by mixing 1-(4-sulfophenyl)-3-methyl-5-pyrazolone with diazonium salt from luminol. The produced dye was assessed using the FT-IR, 1HNMR, and UV-Visible spectroscopy techniques. This dye was dissolved in five polar solvents, and its UV-visible absorption spectra were measured and spectroscopically analysed at room temperature. Additionally, an atomic force microscope (AFM) was used to measure the enhancement of CO3O4 and ZrO2 nanoparticles in luminol azo 1-(4 -sulfophenyl)-3-methyl-5- pyrazolone solutions in aqueous solution.
Keywords
luminol azo 1-(4-sulfophenyl)-3-methyl-5-pyrazolone; synthesis; spectroscopic
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