MORPHOLOGICAL, THERMAL AND ELECTRICAL STUDIES ON CHITOSAN HEAVY METAL COMPLEXES
HUSAIN, M., EL-HADY, M., SAYED, W., HEFNI, H. (2010). MORPHOLOGICAL, THERMAL AND ELECTRICAL STUDIES ON CHITOSAN HEAVY METAL COMPLEXES. EKB Journal Management System, 21(Issue 2-A), 221-238. doi: 10.21608/absb.2010.7377
M. H. HUSAIN; M. F. EL-HADY; W. M. SAYED; H. H. HEFNI. "MORPHOLOGICAL, THERMAL AND ELECTRICAL STUDIES ON CHITOSAN HEAVY METAL COMPLEXES". EKB Journal Management System, 21, Issue 2-A, 2010, 221-238. doi: 10.21608/absb.2010.7377
HUSAIN, M., EL-HADY, M., SAYED, W., HEFNI, H. (2010). 'MORPHOLOGICAL, THERMAL AND ELECTRICAL STUDIES ON CHITOSAN HEAVY METAL COMPLEXES', EKB Journal Management System, 21(Issue 2-A), pp. 221-238. doi: 10.21608/absb.2010.7377
HUSAIN, M., EL-HADY, M., SAYED, W., HEFNI, H. MORPHOLOGICAL, THERMAL AND ELECTRICAL STUDIES ON CHITOSAN HEAVY METAL COMPLEXES. EKB Journal Management System, 2010; 21(Issue 2-A): 221-238. doi: 10.21608/absb.2010.7377

MORPHOLOGICAL, THERMAL AND ELECTRICAL STUDIES ON CHITOSAN HEAVY METAL COMPLEXES

Al-Azhar Bulletin of Science
Article 16, Volume 21, Issue 2-A, December 2010, Page 221-238  XML PDF (1.07 MB)
DOI: 10.21608/absb.2010.7377
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Authors
M. H. HUSAIN email 1; M. F. EL-HADY2; W. M. SAYED1; H. H. HEFNI1
1Polymer lab, Petrochemicals Department, Egyptian Petroleum Research Institute (EPRI).
2Chemistry Department, Faculty of Science, Al-Azhar University, Cairo-Egypt.
Abstract
The chitosan was prepared and mixed with some metal salts (FeCl3, Co(CH3COO)2 and NiCl2) with different concentrations to form chitosan-metal complexes. The characterizations of these complexes were carried out by FTIR and their morphological studies were carried out by scanning electron microscope (SEM) and wide angle X-ray diffraction apparatus. The thermo gravimetric analysis (TGA) and differential scanning calorimetric (DSC) also were carried out. The metal ions which strongly complexed to the amino groups of chitosan like Fe+++ showed a smooth surface product, amorphous phase and thermally more stable than other complexes. The chitosan-metal complexes have a higher electrical conductivity than chitosan compounds at room temperature.
Keywords
morphological; THERMAL; ELECTRICAL STUDIES
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