A:Role of superparamagnetic nanoparticles in magnetic dispersive micro-solid phase extraction | ||||
Records of Pharmaceutical and Biomedical Sciences | ||||
Article 2, Volume 4, Issue 2, July 2020, Page 13-23 PDF (555.79 K) | ||||
Document Type: Mini-reviews | ||||
DOI: 10.21608/rpbs.2020.24931.1055 | ||||
View on SCiNiTO | ||||
Authors | ||||
Hatem Ibrahim Mokhtar 1; Randa Abdel Salam 2; Ghada Hadad 3 | ||||
1R&D, Methodology and stability department, Medical union Pharmaceuticals Co. | ||||
2pharmaceutical analytical chemistry, faculty of pharmacy, Suez Canal University,Ismailia, Egypt | ||||
3Analytical Chemistry Department, Faculty of Pharmacy, Suez Canal University, Ismailia, 41522, Egypt. | ||||
Abstract | ||||
The field of trace analysis of analytes in different samples has gained an increasing interest. This field of analysis gained many benefits by entering the era of nanomaterials and nanotechnologies. One aspect of nanotechnologies influence on the field of trace analysis is the development of magnetic dispersive micro-solid phase extraction (Magnetic D-µ-SPE) technique. Magnetic D-µ-SPE technique involves dispersion of an adsorbent phase with special magnetic properties as finely divided form; usually as nanoparticles, in sample solutions to adsorb target analytes. This is followed by adsorbent retrieval by external magnetic field. This technique provided several advantages including minimal use of solvents and adsorbent materials as well as procedures simplicity. An important key element in the preparation of Magnetic D-µ-SPE adsorbents is tailoring of its magnetic properties. Superparamagnetic nanoparticles had unique properties which fulfilled requirements of Magnetic D-µ-SPE procedures. This review discusses superparamagnetic behavior and its application in preparation of adsorbents for Magnetic D-µ-SPE technique. | ||||
Keywords | ||||
Magnetic dispersive micro-solid phase extraction; Superparamagnetic nanoparticles; Nanoparticles; Trace analysis; Micro-extraction | ||||
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